Materials engineering

Devices and equipment


Mechanical material testing

The mechanical materials testing laboratories are used to analyse material samples to determine their mechanical properties. Materials are tested for strength, ductility, hardness and toughness both at room temperature and under the influence of temperature. In addition, tests can be carried out to determine the fatigue strength in order to evaluate the behaviour of the materials under repeated loading.

TIRA TT28100

  • electromechanical tension and compression testing machine with max. load of 100 kN
  • load cells for 5 kN, 20 kN and 100 kN
  • test area dimensions 1250 x 580 mm
  • measured value acquisition rate up to 5 kHz
  • crosshead travel resolution 0.001 mm
  • crosshead speed 0.01 - 500 mm/min
  • HSR climatic chamber for temperature range from -80°C (liquid nitrogen) to 600°C
  • Maytec HTO-34 high-temperature furnace for max. temperature of 1200°C

Material Test System MTS 810

Hegewald & Peschke KB 30 S

Hegewald & Peschke inspekt 100 table


Non-destructive material testing and materialography

The laboratory for non-destructive material testing offers comprehensive analyses of the quality and integrity of materials. In addition to surface crack testing to detect the finest crack formations, the range of services includes the testing of internal defects using modern methods and dilatometry to determine the thermal expansion and transformation properties of materials. Materialography includes the careful preparation of samples and the creation of micrographs to visualise material structures. Subsequent characterisation provides important insights into the structure, properties and quality of the materials.

Keyence VW-9000

  • modular digital microscope with high-speed camera
  • VH-Z20R standard zoom objective 20x to 200x
  • VH-S30B stand for viewing from any angle with motorised Z-axis
  • multifocus 3D measurement
  • VH-Z250R zoom lens for high magnifications 250x to 2500x
  • VH-S5 vibration-resistant stand for high magnifications
  • VW-600C high-speed colour camera with up to 230,000 fps
     

Leica DMi8 A

  • inverted reflected light and transmitted light microscope with max. magnification of 2000x
  • motorised X-Y stage for oversize images
  • automatic multifocus for high depth of field
  • brightfield, ultra-contrast 3D, darkfield, differential inference, polarisation and fluorescence contrast methods reflected light and phase contrast microscopy transmitted light
  • iMagic IMS analysis software for grain size, phase and particle determination as well as manual image processing and measurement

Bähr Thermoanalyse DIL 802

  • differential dilatometer with a resolution of 0.01 x 10-6 K-1
  • temperature range -160°C to 700°C
  • sample dimensions max. 50 mm length and max. 7 mm diameter
  • max. length changes 4 mm
  • temperature resolution 0.05 K
  • operation under air and inert gas atmosphere
  • contact pressure 0.02 - 1 N adjustable

Calmetrix I-Cal Flex

  • isothermal 8-channel calorimeter for material characterisation, separate measuring cells
  • 20 ml measuring volume per channel with liquid exchange at intervals via pump system
  • continuous pH value measurement
  • low noise and high sensitivity, ideal for weak reactions
  • temperature range from approx. 2°C to 90°C
  • for applications such as polymerisation of plastics, curing of adhesives, corrosion of Mg alloys, battery materials, cement
  • determination of the corrosion rate of Mg alloys via individual pressure measurement per cell

Struers and ATM devices for materialography


Heat treatment

During heat treatment, materials are specifically heated and cooled to change their properties. Precise temperature control is made possible with the help of chamber furnaces and various quenching media. This allows hardness, strength and toughness to be adjusted and adapted to the respective technical requirements.

Nabertherm N 11/H

  • chamber furnace with max. temperature of 1280°C
  • temperature uniformity according to DIN 17052-1 up to +/- 10 K
  • internal dimensions 250 x 350 x 140 mm
  • volume 11 litres
  • parallel swing door opening downwards
  • heating timeTR - 1180°C approx. 320 min
  • controller for precise programming of temperature control

Nabertherm LT 40/12

  • muffle furnace with max. temperature of 1200°C
  • temperature uniformity according to DIN 17052-1 up to +/- 5 K
  • internal dimensions 320 x 490 x 250 mm
  • volume 40 litres
  • parallel swing door opening upwards
  • heating timeTR - 1100°C approx. 97 min
  • controller for precise programming of temperature control
  • protective gas connection for purging the oven with non-flammable process gases

Nabertherm gas flushing and annealing box for N 11/H

  • max. operating temperature of 1100°C
  • ceramic fibre seal
  • gas supply box for non-flammable protective and reaction gases such as argon, nitrogen and forming gas
  • type K batch thermocouple for temperature display or batch control
  • pre-purge rate 15 - 20 l/min and process purge rate 5 - 8 l/min
  • annealing box for carburising and powder nitriding
  • internal dimensions 180 x 290 x 90 mm

iew TTH2t

  • induction heating system with max. output of 2 kW
  • frequency range 70 - 450 kHz
  • various inductor geometries
  • manual operation via push-button and internal cycle operation
  • freely programmable, external temperature control via infrared pyrometer from T > 500°C

Memmert UF110

  • drying oven with working temperature range min. 10 K aboveTR to max. 300°C
  • setting accuracy up to 99.9°C: 0.1 and from 100°C: 0.5
  • interior dimensions 560 x 480 x 400 mm
  • volume 108 litres
  • target time adjustable from 1 min to 99 d
  • adjustable air circulation motor speed, exhaust air flap position, programme run time, time zones, summer/winter time

Scanning electron microscopy and computer tomography

Materials are analysed in detail in the scanning electron microscopy and computed tomography laboratories. The scanning electron microscope enables high-resolution imaging of surface structures and the analysis of chemical compositions. Computed tomography is used for the non-destructive three-dimensional visualisation of internal structures and defects in materials in the micrometre range.

Tescan VEGA

  • scanning electron microscope equipped with SE, BSE and EDX detector
  • acceleration voltage 200 eV - 30 keV
  • infinitely adjustable beam current 1 pA - 2 µA
  • wide-field and high-resolution mode
  • low-vacuum operation for non-conductive or aqueous samples
  • maximum field of view of 7.7 mm at a working distance of 10 mm, more than 50 mm at maximum working distance
  • infinitely variable magnification from 2× to 1,000,000×
  • maximum sample dimensions of 54 (H) x 145 (X) × 145 (Y) mm

Edwards Sputter Coater S150B

  • coating of non-conductive samples for SEM examinations
  • process pressure 10-3 mbar
  • current 0 - 50 mA stepless
  • voltage 0 - 1.5 kV
  • maximum sample area 50 x 50 mm2
  • sample area for high homogeneity 5 x 5 mm2

Bruker Skyscan 2214

  • multiscale 3D X-ray nanotomography (XRM) with resolution in the sub-micrometre range
  • objects up to Ø 300 mm and length up to approx. 400 mm
  • modular flat-panel and CCD detector design with filter magazine depending on material and application
  • very fine nanofocus X-ray source (< 500 nm voxel size)
  • W (tungsten) and LaB6 (lanthanum hexaboride) filaments
  • acceleration voltage from 20 - 160 kV
  • maximum power of 16 W
  • software-supported image acquisition, 3D reconstruction and analysis

Contact persons for the field of materials technology

Prof. Dr.-Ing.
Petra Maier

Werkstoff- und Fertigungstechnik | Prodekanin | Gleichstellungsbeauftragte der Fakultät

Tel:

Tel: +49 3831 45 6914

Room:

Raum 17 / Haus W9 | BFW

Dekan der Fakultät für Maschinenbau
Dekan der Fakultät für Maschinenbau
Dekan der Fakultät für Maschinenbau

Prof. Dr.-Ing.
Roy Keipke

Werkstofftechnik, Konstruktion | Praktikumsbeauftragter

Tel:

+49 3831 45 6778

Room:

Raum 20 / Haus W9 | BFW

Katja Putzig

Laboringenieurin

Tel:

+49 3831 45 6560

Room:

122b, Haus 20